TABLE 1

Rf Values for Investigated Mobile Phases Using Silica Gel 60 or ITLC Silica Gel Plates as Stationary Phase

Silica gel 60ITLC silica gel
No.Mobile phaseRf (68Ga)Rf (68Ga-PSMA)MinutesRf (68Ga)Rf (68Ga-PSMA)Minutes
10.1 M Na3C6H5O7 (pH 4)0.9–10.1200.9–10.7–0.8
2MeOH/NH4OAc (1:1)00.8–0.92300.8–0.97
35% NaCl/MeOH/25% NH3 (3:1:1)0118015
4MeOH/0.9% NaCl (9:1)01
5MeOH/0.9% NaCl/1 (mg/mL) EDTA (9:1:0.5)0–0.11250.9–10.9
6MeCN/H2O (1:1)0–10–1
7Cyclohexanone/2 M HCl (20:1)00
  • Development times are given only for applicable solvent systems.